Publications
NIBIOs employees contribute to several hundred scientific articles and research reports every year. You can browse or search in our collection which contains references and links to these publications as well as other research and dissemination activities. The collection is continously updated with new and historical material.
2006
Abstract
The aim of this study was to compare two methods for non-destructive strength testing of wood by the use of dynamic modulus of elasticity (MOEdyn). The two methods are based on resonant vibration excitation and ultrasonic pulse excitation. Sound Pinus sylvestris L. sapwood samples treated with two copper-containing wood preservatives and two chitosan solutions were evaluated at two moisture levels. There was a significant correlation between the measurements given by the two MOEdyn test devices. An analysis of variance showed significant differences between the different treatments and between different moisture levels. Potential use of the non-destructive MOEdyn methods in durability testing is discussed.
Abstract
There is a high correlation between methods for dynamic modulus of elasticity (MOEdyn) and static modulus of elasticity (MOEstat). MOEdyn methods have been found sensitive to detect early stages of decay and may be seen as an option for non-destructive wood durability testing.As the MOEstat measurements do not change after reaching the fibre saturation point, the uncorrected MOEdyn data from ultrasonic pulse excitation method provides increasin values after fibre saturation. This is due to the effect of free water in the cell lumen on ultrasonic waves. The aim of this study was to make a moisture calibration for the MOEdyn ultrasonic pulse excitation method using Scots pine (Pinus sylvestris L.) sapwood samples.MOE was measured at five different moisture levels. Three different MOE test methods were used: MOEdyn using ultrasound and vibration excitation and the traditional MOEstat. Sound Scots pine sapwood samples treated with two copper-containing wood preservatives and two chitosan solutions were evaluated, using untreated sapwood samples as control.In this study a correction value (\"k\") was calculated based on data from different moisture levels for water saturated samples using four different wood treatments and control. By measuring MOEdyn ultrasonic at wood moisture contents just below fibre saturation point, a minor effect of incipient water accumulation in the wood matrix was detected.Wood treatments influence the \"k\" value, and a \"k\" value needs to be calculated for all wood treatments when measuring MOEdyn ultrasound above fibre saturation. All the three MOE test methods in this study are applicable for all wood moisture levels as long as a \"k\" value is calculated for MOEdyn ultrasound above fibre saturation.
Abstract
A method for quantitative determination of extractives from heartwood of Scots pine (Pinus sylvestris L.) using gas chromatography (GC) with flame ionization detection (FID) was developed. The limit of detection (LOD) was 0.03mg/g wood and the linear range (r=0.9994) was up to 10mg/g with accuracy within ±10% and precision of 18% relative standard deviation. The identification of the extractives was performed using gas chromatography combined with mass spectrometry (GC–MS). The yields of extraction by Soxhlet were tested for solid wood, small particles and fine powder. Small particles were chosen for further analysis. This treatment gave good yields of the most important extractives: pinosylvin, pinosylvin monomethyl ether, resin acids and free fatty acids. The method is used to demonstrate the variation of these extractives across stems and differences in north–south direction.
Abstract
When using chitosan as an antifungal agent in wood it is important to understand which factors contribute to a higher fixation ratio to optimize the utilization of chitosan, the active component. Small pine samples were impregnated with chitosan solutions varying in molecular weight, concentration, pH, polymerization agent, acid and degree of deacetylation. Different post-treatments such as time, temperature, moisture content and the effect of present air were applied to the samples to evaluate the effect on the relative retention. After impregnation, the samples, with a volume of 1.5 cm3, were leached in separate test-tubes according to EN-84. The samples were prepared in a paired design where both samples were impregnated, but only one was leached. Both leached and unleached samples were analysed for their chitosan content, and the relative ratio was used as a measure for the relative retention of chitosan during leaching. The results from these trials show that pH in the range of 5.1-5.9 is favourable. The molecular weight should be as high as possible yet able to penetrate the wood structure, and the use of acetic acid gives far better fixation than the use of hydrochloric acid.
Authors
Erik LarnøyAbstract
No abstract has been registered
Authors
Andreas TreuAbstract
No abstract has been registered
Abstract
Resins and oils can easily evaporate during drying processes at high temperatures. The aim of this research was to investigate different drying methods such as oven-drying, vacuumdrying and freeze-drying of resin modified pine-sapwood samples to determine wood moisture content (MC) and weight percent gain (WPG). The results showed that freeze-drying is the slowest process. Vacuum drying of water impregnated samples takes approx. 7 times longer compared to oven-drying. The initial moisture content of wood before impregnation used in this research has only little influence on the WPG.
Authors
Andreas TreuAbstract
No abstract has been registered
Abstract
This study evaluates the decay and termite resistance of Scots pine (Pinus sylvestris L.) treated with 4-methoxytrityl tetrafluoroborate (MTFB).Decay resistance tests of unleached samples showed that 2%, 1.5% and 1% concentrations of MTFB (15.4kg/m3, 11.1kg/m3, and 7.4kg/m3, retention levels, respectively) gave less than 2% decay of Postia placenta and concentrations of 2% and 1.5% less than 2% decay of Coniophora puteana.Wood specimens treated with 4-methoxytrityl tetrafluoroborate solutions were not protected against the brown rot fungi after a 14-day severe leaching process, suggesting excessive leaching of the chemical from wood. Treatment with 2% concentration protected against subterranean termites, Coptotermes formosanus Shiraki based on mass losses in both leached and unleached wood specimens in comparison with lower concentration levels.These results suggest that 4-methoxytrityl tetrafluoroborate might be promising to protect wood being used outdoors against termite attack. However, 4-methoxytrityl tetrafluoroborate did not protect wood against fungal decay. Field tests are needed to observe the performance of 4-methoxytrityl tetrafluoroborate treated wood in ground contact.
Abstract
In Norway exterior wood structures have traditionally nearly exclusively been made of treated and untreated Norway spruce (Picea abies (L.) Karst) and Scots pine (Pinus sylvestris L.). In recent years there has been a tendency that other tree species, like various domestic hardwoods and imported species have been used in exterior above ground applications, often unfinished. For several wood species, especially hardwoods, information regarding the durability in use class 3 is lacking. The test procedures prescribed in the European standards, both laboratory and field tests, have some weaknesses regarding to natural durability testing. Hence, some new methods for accelerated above ground testing have been put forward. The main objectives of this project are to evaluate natural durability of Norwegian wood species for above ground applications, and to study various methods for assessing decay in wood. This paper presents the material and methods used in the project, and report the results from double layer tests after one year of exposure. No decay was detected, but almost all wood species were considerably discoloured. Thuja (Norw.), Thuja (Am.), Intsia and Tectona had the least amount of discolouration. The Norwegian softwood species had generally less discolouration than the Norwegian hardwood species. CCA and Cu preservative impregnated and FA modified Pinus sylvestris sapwood had more cracks than most of the untreated wood species. Moreover, some of the Picea abies qualities and Pinus sylvestris sapwood samples had substantial amounts of cracks.